Method 7303

Elements by ICP


This method is for the collection and analysis of elements (metals).  The sample is collected on a 0.8 micron cellulose ester membrane.  The filter is digested using concentrated hydrochloric acid (HCl) and concentrated nitric acid (HNO3), and after digestion the sample is analyzed using ICP (inductively coupled plasma).  

The working range of this method is up to 100 mg/m³ for each element in a 500L air sample.

NOTE: This method is similar to NIOSH Method 7301 differing only in the use of the hot block for the digestions of the sampler.


(NIOSH Issue 2: 15 August 1994)

Request-A-Quote

No Obligation Quotation for Analytical Services

If you would like us to provide a quote for laboratory analysis, just provide us with as much information as you can about your project (the more, the better) and we'll provide you a quote via email. As you are searching or browsing our Analytical Guide, you'll see the Request-A-Quote icon... just click on it to start the request process.
Request-A-Quote

Method Data

Hold Times, Preservatives, Preps, Collection, Analytical & Documentation
Holding Time:   None specified by the method.
Preservatives:   None specified by the method.
Required Preps:   37mm cellulose ester membrane filter
Collection Method:   The method recommends a 1-4 L/min. flow rate. The sample collection volume varies by element, refer to Table 1 of the method.
Analytical Methodology:   ICP
Documentation:   7303

Analyte List*

Analyte Formula CAS Number Detection Limit
Calcium oxide
CaO
1305-78-8
11.6
 µg
Magnesium oxide
MgO
1309-48-4
5.75
 µg
Zinc oxide
ZnO
1314-13-2
2.05
 µg
Tellurium
Te
13494-80-9
12.5
 µg
Aluminum
Al
7429-90-5
9.25
 µg
Iron
Fe
7439-89-6
5
 µg
Lead
Pb
7439-92-1
1.75
 µg
Magnesium
Mg
7439-95-4
3.5
 µg
Manganese
Mn
7439-96-5
0.1
 µg
Molybdenum
Mo
7439-98-7
0.6
 µg
Neodymium
Nd
7440-00-8
0.75
 µg
Nickel
Ni
7440-02-0
0.98
 µg
Palladium
Pd
7440-05-3
0.75
 µg
Platinum
Pt
7440-06-4
0.38
 µg
Strontium
Sr
7440-24-6
0.15
 µg
Thallium
Tl
7440-28-0
3.32
 µg
Tin
Sn
7440-31-5
1.25
 µg
Titanium
Ti
7440-32-6
0.4
 µg
Antimony
Sb
7440-36-0
1.5
 µg
Arsenic
As
7440-38-2
0.075
 µg
Barium
Ba
7440-39-3
0.006
 µg
Beryllium
Be
7440-41-7
0.062
 µg
Boron
B
7440-42-8
0.71
 µg
Cadmium
Cd
7440-43-9
0.3
 µg
Chromium
Cr
7440-47-3
0.75
 µg
Cobalt
Co
7440-48-4
0.27
 µg
Copper
Cu
7440-50-8
1.5
 µg
Gallium
Ga
7440-55-3
2.25
 µg
Gold
Au
7440-57-5
1.25
 µg
Vanadium
V
7440-62-2
0.25
 µg
Yttrium
Y
7440-65-5
0.075
 µg
Zinc
Zn
7440-66-6
1.65
 µg
Bismuth
Bi
7440-69-9
2.12
 µg
Calcium
Ca
7440-70-2
8.25
 µg
Indium
In
7440-74-6
1.25
 µg
Phosphorus
P
7723-14-0
25
 µg
Selenium
Se
7782-49-2
1.6
 µg

* The analytes and detection limits listed for each method represent the typical detection limits and analytes reported for that particular method. Keep in mind that analyte lists may vary from laboratory to laboratory. Detection limits may also vary from lab to lab and are dependent upon the sample size, matrix, and any interferences that may be present in the sample.