This method is for the collection and analysis of oxalic acid from workplace air. The sample is collected on a glass fiber filter. After sample collection the extracted with 10mLs of a misture of 0.028M sodium hydroxide (NaOH) and analyzed by ion chromatography (IC).
NOTE: This is a partically validated method.
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Hold Times, Preservatives, Preps, Collection, Analytical & Documentation | |
---|---|
Holding Time: | Recoveries of oxalic acid were good after storage of 28 days at ambient temperatures. |
Preservatives: | None specified in the method. |
Required Preps: | 37mm MCE filter |
Collection Method: | The method recommends a 1.0 L/min. flow rate with a 100L sample collection volume. |
Analytical Methodology: | IC |
Documentation: | PV2115 |
Analyte | Formula | CAS Number | Detection Limit | |
---|---|---|---|---|
Oxalic acid | C2H2O4 |
144-62-7 |
10 |
ug |
* The analytes and detection limits listed for each method represent the typical detection limits and analytes reported for that particular method. Keep in mind that analyte lists may vary from laboratory to laboratory. Detection limits may also vary from lab to lab and are dependent upon the sample size, matrix, and any interferences that may be present in the sample.