This method describes the sample collection and analysis of desflurane. Samples are collected by drawing a known volume of air through standard size Anasorb 747 tubes. Samples are desorbed with toluene and analyzed by GC using a flame ionization detector (FID).
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| Hold Times, Preservatives, Preps, Collection, Analytical & Documentation | |
|---|---|
| Holding Time: | The recovery of analyte from the collection medium after storage must be 75% or greater. Recoveries of greater than 94% were obtained from samples stored for up to 16 days at both ambient (22°C) and cool (4°C) temperatures. |
| Preservatives: | Store at ambient (22°C) or cool (4°C) temperatures. |
| Required Preps: | Anasorb 747 tube: 140 mg/70 mg, 7cm x 6mm OD x 4mm ID |
| Collection Method: | Anasorb 747: 3 L at 0.05 L/min. |
| Analytical Methodology: | GC/FID |
| Documentation: | 
106
|
| Analyte | Formula | CAS Number | Detection Limit | |
|---|---|---|---|---|
| Desflurane | 57041-67-5 |
0.205 |
µg | |
* The analytes and detection limits listed for each method represent the typical detection limits and analytes reported for that particular method. Keep in mind that analyte lists may vary from laboratory to laboratory. Detection limits may also vary from lab to lab and are dependent upon the sample size, matrix, and any interferences that may be present in the sample.