This method describes the sample collection and analysis of propylene oxide. Samples are collected by drawing air through standard size Anasorb 747 adsorbent tubes. The Anasorb 747 is desorbed with carbon disulfide and the desorbate is analyzed by gas chromatography using a flame ionization detector.
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Hold Times, Preservatives, Preps, Collection, Analytical & Documentation | |
---|---|
Holding Time: | Up to 15 days. |
Preservatives: | Stored samples should be kept at 0°C or colder to reduce migration. Reduced temperature shipment of samples to the laboratory is not necessary. |
Required Preps: | Samples are collected with solid sorbent sampling tubes containing Anasorb 747: 140mg/70mg. Each tube consists of two sections of Anasorb 747 separated by a urethane foam plug. |
Collection Method: | Anasorb 747 tube: 5 L at 0.1 L/min. |
Analytical Methodology: | GC/FID. |
Documentation: | 088 |
Analyte | Formula | CAS Number | Detection Limit | |
---|---|---|---|---|
Propylene oxide | C3H6O |
75-56-9 |
0.415 |
µg |
* The analytes and detection limits listed for each method represent the typical detection limits and analytes reported for that particular method. Keep in mind that analyte lists may vary from laboratory to laboratory. Detection limits may also vary from lab to lab and are dependent upon the sample size, matrix, and any interferences that may be present in the sample.